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Department : Kimya Mühendisliği B ... ✕
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Benzotiyofen@Pd as an efficient and stable catalyst for the electrocatalytic oxidation of hydrazine

Hilal DEMİR KIVRAK

An efficient methods for the synthesis of 2-(2,5-dimethylphenyl)-3-iodobenzo[b]thiophene (4) is described, and investigated its anode catalyst performance by using electrochemical methods (CV, CA and EIS). When 2-(2,5dimethylphenyl)-3-iodobenzo[b]thiophene (4) is applied, the specific activity is found as 25.811 mA/cm(2). Interestingly, when Palladium (Pd) is electrochemically deposited on the benzothiophene derivative, the catalytic activity increased the 80.930 mA/cm(2). This result is highest than the current metal based anode catalyst. Moreover, EIS and CA measurements display that Pd dope ...More

Article 2022 Mühendislik Fakültesi Fuel328 61 Views
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A novel carbohydrate antigen 125 electrochemical sensor based on sweet almond oil organo-hydrogels

Nahit AKTAŞ

Ovarian cancer is a gynecological disease causing many deaths among women around the world. Carbohydrate antigen 125 (CA-125) is a single biomarker known to be a tumor marker of ovarian cancer. CA-125 is widely used to monitor the treatment process, recurrences, and for the detection of ovarian cancer. Herein, organo-hydrogels were prepared in order to detect CA-125 sensitively in serum medium with electrochemical methods. Organo-hydrogels were obtained by the free radical polymerization reaction using agar and glycerol with varying proportions of sweet almond oil using methylene bisacrylamide ...More

Article 2023 Mühendislik Fakültesi Materials Chemistry and Physics298 52 Views
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Carbon Nanotube Supported CdM(S, Se)/CdTe Anode Catalysts for Electrooxidation of Glucose in Alkaline Media

Hilal DEMİR KIVRAK | Nahit AKTAŞ

The sequential sodium borohydride (SBH, NaBH4) reduction method was utilized to prepare the 0.1 CdSe/CNT, 0.1 CdS/CNT, 0.1 (CdS-CNT)/CdTe, and 0.1 (CdSe-CNT)/CdTe catalysts. The XRD, SEM-EDS, TEM, and XPS analyses were used to characterize the catalysts. The electrochemical measurements were examined by cyclic voltammetry (CV), chronoamperometry (CA), and electrochemical impedance spectroscopy (EIS) analyses for glucose electrooxidation. The characterization analyses revealed that the desired structure was formed on the support material. The electrochemical analysis results indicated that the ...More

Article 2023 Mühendislik Fakültesi ChemistrySelect8 ( 12 ) 75 Views
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Fabrication of molecularly imprinted cotton fibers for quantification of streptomycin in honey samples

Nahit AKTAŞ

Streptomycin is a type of aminoglycoside used in treatment of several infections and with serious side effects in humans and animals, such as ototoxicity and nephrotoxicity. In the present study, we focused on the preparation of streptomycin-imprinted cotton fiber for rapid, sensitive and selective quantification of streptomycin in honey samples. The imprinted cotton fibers were characterized by attenuated total reflectance-Fourier transform spectroscopy, scanning electron microscopy, and x-ray photoelectron spectroscopy. In addition, the imprinted cotton fibers showed high adsorption capacity ...More

Article 2023 Mühendislik Fakültesi Journal of Applied Polymer Science140 ( 28 ) 53 Views
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Characterization of p(PmO), p(LO) and p(RO) organoparticles, their bioactivity properties and their effect on pancreatic cancer Capan-1 cell

Nahit AKTAŞ

For the first time in the literature, p (PmO), p (LO) and p (RO) organo-particles were synthesized from Peppermint oil, Lemon oil and Rose oil. Of the organo-particles L-929 cell line viability/cytotoxicity and anticancer effect against Capan-1 pancreatic cancer cell line were investigated. p (PmO), p (LO) and p (RO) organo-particles were featured by thermogravimetry (TGA), Fourier Transform Infrared Spectroscopy (FTIR), Scanning electron microscope (SEM), Particle size (DLS), and particle charge (zeta potential, Zeta) analyses. Antioxidant, biocompatible, and antimicrobial activities and in v ...More

Article 2023 Mühendislik Fakültesi Materials Chemistry and Physics305 41 Views
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The advanced polymer composite coated fabrics as an anode electrode and photocatalytic glucose micro fuel cell design

Hilal DEMİR KIVRAK

At present, poly N-isopropyl acrylamide (PNIPAM) polymer composites containing titanium dioxide (TiO2) and carbon-TiO2 (C-TiO2) were designed for photocatalytic glucose electrooxidation by coating the textile fabric surface such as wool blended fabrics called Sign Cocana (SC), Valencia (VC), Dante (DT), and Broadway (BW). C-TiO2 was obtained from TiO2 in a furnace under hexane gas with a certain temperature and time. Polymer synthesis was realized by a polymerization method. The surface analyses of these polymer composite fabric electrodes were characterized by scanning electron microscopy-ene ...More

Article 2023 Mühendislik Fakültesi Journal of Photochemistry and Photobiology A: Chemistry444 15 Views
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p(thyme oil) and p(clove oil) organo-particles with biocompatible, anticancer, antioxidant, and antibacterial properties against Capan-1 and L-929 cells

Nahit AKTAŞ

The synthesis of p(ClO) and p(TO) organo-particles from clove oil and thyme oil is the first in the literature. The particles were tested against the L-929 cell line for cell viability/cytotoxicity. The anticancer activity was studied against the Capan-1 pancreatic cancer cell line. p(ClO) and p(TO) organo-particles were featured by thermogravimetry (TGA), Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), particle size (DLS), and particle charge (zeta potential, Zeta) analyses. Antioxidant, biocompatible, antimicrobial, and in vitro cytotoxicity specialties w ...More

Article 2023 Mühendislik Fakültesi Canadian Journal of Chemical Engineering102 ( 1 ) 30 Views
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Evaluation of particle biosynthesis, p(Okra) particle bioactivity, and drug release properties using Abelmoschus esculentus (okra) plant extract

Nahit AKTAŞ

Interest in synthesizing functional materials from natural compounds has increased recently. For this reason, compound particles attract attention due to their multifunctional properties. Abelmoschus esculentus L. (Okra) is a vegetable species belonging to the Hibiscus family, widely used for its edible unripe fruit. This study synthesized the particle from the Abelmoschus esculentus (Okra) extract (Oe) by emulsion polymerization. In this synthesis, ammonium persulfate (APS, initiator) to form free radicals at the Abelmoschus esculentus (Okra) extract (Oe) and ethylene glycol di methacrylate t ...More

Article 2023 Mühendislik Fakültesi Polymer Bulletin81 ( 5 ) 36 Views
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The enhanced TiO2-supported CdTe photocatalysts for photocatalytic hydrogen peroxide electrooxidation

Nahit AKTAŞ

At present, titanium dioxide (TiO2)-supported CdTe photocatalysts were prepared by wet impregnation method for photocatalytic hydrogen peroxide (H2O2) electrooxidation. The structural and morphology surface analyses of these photocatalysts were characterized by X-Ray diffraction (XRD), scanning electron microscopy-energy dispersive X-Ray (SEM-EDX) and mapping analysis, high-resolution transmission electron microscopy (HR-TEM), ultraviolet–visible (UV–VIS) spectroscopy, X-ray photoelectron spectroscopy (XPS), and inductively coupled plasma mass spectrometry (ICP-MS). In addition, the photocatal ...More

Article 2023 Mühendislik Fakültesi Journal of Photochemistry and Photobiology A: Chemistry445 55 Views
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Properties of ZnO and Zn Nanoparticles Produced by Electrical Discharge in Liquid Method

Emil ÖMÜRZAK

The physical processes used to synthesize nanoparticles today are labor-intensive and inefficient in terms of energy use. Our approach, which we employed to create nanoparticles, is straightforward and economical. Using this technique, we synthesized Zinc Oxide (ZnO) nanoparticles and investigated their characteristics using several characterization techniques. We can regulate the form and size of our nanoparticles by altering the experimental conditions, as demonstrated by our investigations. This demonstrates the importance of experimental parameters in synthesizing ZnO nanoparticles by this ...More

Proceedings Paper 2022 Mühendislik Fakültesi International Exchange and Innovation Conference on Engineering and Sciences8 14 Views
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Optimization by Using the Taguchi Method of Boric Acid Production by Dissolving Flash Calcined Colemanite in Water Saturated with SO2

Ali Osman SOLAK

Turkey has the largest boron reserves in the world with a rate of approximately 72. The most common commercial boron reserves in Turkey are colemanite, tincal, and ulexite. Boric acid, which is the most commonly used boron compound in Turkey, is obtained from the dissolution of colemanite with sulfuric acid. In the present study, an aqueous medium saturated with sulfur dioxide instead of sulfuric acid was used in order to obtain boric acid. Colemanite ore was flash calcined at various temperatures and optimum dissolution conditions of the ore obtained in water saturated with SO2 were examined ...More

Article 2023 Mühendislik Fakültesi Iranian Journal of Chemistry and Chemical Engineering (IJCCE)42 ( 5 ) 17 Views
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The efficiency of cationic-based hydrogels in heavy metal removal from wastewater

Bakıt BORKOYEV | Kalıypa SALİYEVA

The present study draws attention to arsenic (V) (As(V)), chromium (III) (Cr(III)), and chromium (VI) (Cr(VI)) heavy metal pollutants, which have negative effects on aquatic ecosystems and indirectly pose a serious threat to the health of living things in the environment. Homopolymer and copolymer hydrogels were synthesized by the UV polymerization technique using 2-acrylamido-2-methyl-1-propansulfonic acid sodium salt (AMPS) and 3-acrlylamidopropil-trimethyl ammonium chloride monomers, and a crosslinker aimed to improve the swelling properties and metal sorption of the prepared hydrogels. The ...More

Article 2023 Mühendislik Fakültesi Polymer Bulletin ( Published online: 21 November 2023 ) 31 Views
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