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Found: 43 Piece 0.001 sn
UN Sustainable Development : Good health and well ... ✕Databases : Sciencedirect ✕
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Good health and well-beingEnsure healthy lives and promote well-being for all ages
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A novel carbohydrate antigen 125 electrochemical sensor based on sweet almond oil organo-hydrogels

Nahit AKTAŞ

Ovarian cancer is a gynecological disease causing many deaths among women around the world. Carbohydrate antigen 125 (CA-125) is a single biomarker known to be a tumor marker of ovarian cancer. CA-125 is widely used to monitor the treatment process, recurrences, and for the detection of ovarian cancer. Herein, organo-hydrogels were prepared in order to detect CA-125 sensitively in serum medium with electrochemical methods. Organo-hydrogels were obtained by the free radical polymerization reaction using agar and glycerol with varying proportions of sweet almond oil using methylene bisacrylamide ...More

Article 2023 Mühendislik Fakültesi Materials Chemistry and Physics298 52 Views
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Electrochemical oxidation of perfluorooctanesulfonate (PFOS) from simulated soil leachate and landfill leachate concentrate

Mehmet KOBYA

The near-widespread presence of poly- and perfluoroalkyl substances (PFASs) in humans has generated concerns regarding the potential negative impact of these chemicals on human health, as some PFASs are exceedingly persistent and bioaccumulative. Among the perfluorinated PFASs, which exhibit high polarity and strong carbon–fluorine bonds, perfluorooctanesulfonate (PFOS) is one of the frequently encountered species. In this study, the efficiency of electrooxidation (EO) and its application in groundwater simulation were first evaluated as a realistic approach to PFOS removal. After optimizing E ...More

Article 2023 Mühendislik Fakültesi Journal of Water Process Engineering56 11 Views
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Three novel 1,2,3-triazole-fused compounds: Syntheses, structural and spectroscopic characterizations with molecular modeling

Ferhan TÜMER

In this study, we report syntheses, structural and spectroscopic characterizations, and molecular modeling of three novel triazole fused compounds: 4-((4-methoxyphenoxy)methyl)-1-(4-methoxyphenyl)-1H-1,2,3-triazole, 1-(4-isopropylphenyl)-4-((4-methoxyphenoxy)methyl)-1H-1,2,3-triazole, and 1-(4-fluorophenyl)-4-((4-methoxyphenoxy)methyl)-1H-1,2,3-triazole. Their molecular structures and intermolecular interactions were elucidated using single-crystal X-ray crystallography. The compounds crystallize in the P-1 and P21/c space groups with weak C−H∙∙∙N and C-H∙∙∙O interactions. Hirshfeld surface an ...More

Article 2023 Mühendislik Fakültesi Journal of Molecular Structure1299 17 Views
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Investigation of changes in chemical composition and rheological properties of Kyrgyz rice cultivars (Ozgon rice) depending on long-term stack-storage after harvesting

Camilya SMANALİYEVA | Kalıypa SALİYEVA | Bakıt BORKOYEV

The present work investigated the effect of long-term stack-storage after harvesting on selected chemical and rheological properties of Kyrgyz rice cultivars, Ozgon. The performance indicators of in stack-stored Ozgon rice samples after 4, 6, and 12 days was grain size, grain weight, color, moisture, total starch, amylose, protein, fat and ash contents, and mineral composition as well as the rheological properties of rice flour dough. The change of stored rice is caused by the organic modification of the starch structure, decreasing of moisture as well as proteolysis of proteins in the endospe ...More

Article 2015 Mühendislik Fakültesi LWT - Food Science and Technology63 ( 1 ) 187 Views
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Amino Acid and Fatty Acid Profile of the Mare's Milk Produced on Suusamyr Pastures of the Kyrgyz Republic During Lactation Period

Ayçürök MACİTOVA | Asılbek KULMIRZAYEV | Cıldızay ÖZBEKOVA | Aybek BODOŞOV

The high nutritional and health-promoting properties of kymyz, a traditional drink of nomads produced from mare's milk, are well-known and reported in literature. The composition of mare's milk is significantly different from that of cow and other ruminants. Fatty acid composition and amino acid profile of mare's milk produced at Suusamyr pastures of Kyrgyzstan were studied during four lactation months (May, June, July and August). The amino acid composition was determined by precolumn derivatization with diethyl ethoxymethylenemalonate (DEEMM) in high-performance liquid chromatography (HPLC) ...More

Proceedings Paper 2015 Mühendislik Fakültesi Procedia - Social and Behavioral Sciences195 83 Views
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Phosphorus-nitrogen compounds: part 30. Syntheses and structural investigations, antimicrobial and cytotoxic activities and DNA interactions of vanillinato-substituted NN or NO spirocyclic monoferrocenyl cyclotriphosphazenes

Ali Osman SOLAK

The gradual Cl replacement reactions of NN (1–3) or NO spirocyclic monoferrocenyl cyclotriphosphazenes (4 and 5) with the potassium salt of 4-hydroxy-3-methoxybenzaldehyde (potassium vanillinate) resulted in the mono (1a–5a), geminal (gem-1b–5b), non-geminal (cis-5b and trans -1b–4b), tri (1c, 3c–5c) and tetra-vanillinato-substituted phosphazenes (1d–5d). All the phosphazene derivatives have stereogenic P-center(s), except tetra-substituted ones. The vanillinatophosphazenes have reversible voltammograms with one-electron anodic and cathodic peaks which are attributed to ferrocenyl redox probe. ...More

Article 2015 Mühendislik Fakültesi JBIC : Journal of Biological Inorganic Chemistry20 ( 1 ) 80 Views
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Electrochemically modified sulfisoxazole nanofilm on glassy carbon for determination of cadmium(II) in water samples

Ali Osman SOLAK

Sulfisoxazole (SO) was grafted to glassy carbon electrode (GCE) via the electrochemical oxidation of SO in acetonitrile solution containing 0.1 M tetrabutylammoniumtetra-fluoroborate (TBATFB). The prepared electrode was characterized by using cyclic voltammetry (CV), electrochemical impedance spectroscopy (EIS), reflection–absorption infrared spectroscopy (RAIRS) and X-ray photoelectron spectroscopy (XPS). The ellipsometric thickness of SO nanofilm at the glassy carbon surface was obtained as 14.48 ± 0.11 nm. The stability of the SO modified GCE was studied. The SO modified GCE was also utiliz ...More

Article 2013 Mühendislik Fakültesi Electrochimica Acta105 63 Views
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A novel voltammetric sensor based on p-aminothiophenol functionalized graphene oxide/gold nanoparticles for determining quercetin in the presence of ascorbic acid

Ali Osman SOLAK

In this study, gold nanoparticles (AuNPs) with the diameters of maximum 25 nm were self-assembled onto the surfaces of p-aminothiophenol functionalized graphene oxide (ATPGO) sheets simply by mixing their aqueous dispersions. The prepared graphene oxide (GO), ATPGO and AuNPs–ATPGO composites were characterized by a transmission electron microscope (TEM), X-ray photoelectron spectroscopy (XPS), reflection–absorption infrared spectroscopy (RAIRS), the X-ray diffraction (XRD) method and Raman spectroscopy. The electrochemical determination of quercetin (QR) has been studied using square wave volt ...More

Article 2013 Mühendislik Fakültesi Journal of Electroanalytical Chemistry698 76 Views
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Surface characterization of dinitrophenyl-diaminophenyl nanoplatform on glassy carbon

Ali Osman SOLAK

2,4-dinitrophenol (DNP) was covalently bonded to glassy carbon substrate by cyclic voltammetry (CV) technique. 2, 4-diaminophenol film (DAPO) was acquired with electrochemical reduction of 2,4-dinitrophenol film (DNPO). Prepared films were characterized by X-ray photoelectron spectroscopy (XPS) and germanium attenuated total reflection infrared (GATR-FT-IR) spectroscopy. A hemispherical germanium ATR element used with p-polarized light at 65° incidence angle yielded high signal/noise IR spectra for monolayer coverage of molecules on glassy carbon substrate. Layer thickness of films was measure ...More

Article 2013 Mühendislik Fakültesi Journal of Molecular Liquids187 52 Views
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A novel sensitive Cu(II) and Cd(II) nanosensor platform: Graphene oxide terminated p-aminophenyl modified glassy carbon surface

Ali Osman SOLAK

Graphene oxide (GO) based glassy carbon (GC) electrode has been prepared. Firstly, p-nitrophenyl (NP) modified GC (NP/GC) electrode was prepared via the electrochemical reduction of its tetraflouroborate diazonium salt. After the formation of NP/GC electrode, the negative potential was applied to NP/GC electrode to reduce the nitro groups to amine. p-Aminophenyl (AP) modified GC (AP/GC) electrode was immersed into a graphene oxide solution containing 1-ethyl-3(3-(dimethlyamino)propyl)-carbodiimide. Hence, we constructed GO terminated AP modified GC (GO/AP/GC) electrode. NP/GC, AP/GC and GO/AP/ ...More

Proceedings Paper 2013 Mühendislik Fakültesi Electrochimica Acta112 78 Views
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A novel impedimetric biosensor based on graphene oxide/gold nanoplatform for detection of DNA arrays

Ali Osman SOLAK

A highly sensitive method for detection of DNA hybridization was developed. This method was based on the modification of glassy carbon electrode with gold nanoparticles (AuNPs) involving p-aminothiophenol (ATP) functionalized graphene oxide (GO). This GO was used as a platform for impedimetric genosensing using 5′-TA GGG CCA CTT GGA CCT-(CH2)3-SH-3′ single-stranded probe (ss-DNA), 5′-AGG TCC AAG TGG CCC TA-3′ (target DNA), 5′-SH-C6-TAG GGC CA-3′ (non-complementary-1) and 5′-SH-C6-TGC CCG TTA CG 3-′ (non-complementary-2) oligonucleotide sequences. The film exhibited excellent properties for imm ...More

Article 2013 Mühendislik Fakültesi Sensors and Actuators B: Chemical188 106 Views
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Phosphorus-nitrogen compounds: Part 28. Syntheses, structural characterizations, antimicrobial and cytotoxic activities, and DNA interactions of new phosphazenes bearing vanillinato and pendant ferrocenyl groups

Ali Osman SOLAK

The gradually Cl replacement reactions of spirocyclic mono (1 and 2) and bisferrocenyl cyclotriphosphazenes (3–5) with the potassium salt of 4-hydroxy-3-methoxybenzaldehyde (potassium vanillinate) gave mono (1a–5a), geminal (gem-1b–5b), non-geminal (cis-1b, cis-5b and trans-2b–5b), tri (1c–5c) and tetra-substituted phosphazenes (1d–5d). Some phosphazenes have stereogenic P-center(s). The chirality of 4c was verified using chiral HPLC column. Electrochemical behaviors were influenced only by the number of ferrocene groups, but not the length of the amine chains and the substituent(s). The struc ...More

Article 2013 Mühendislik Fakültesi Journal of Molecular Structure1049 65 Views
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