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Найденный: 5 Экземпляр 0.001 sn
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Properties of ZnO and Zn Nanoparticles Produced by Electrical Discharge in Liquid Method

Emil ÖMÜRZAK

The physical processes used to synthesize nanoparticles today are labor-intensive and inefficient in terms of energy use. Our approach, which we employed to create nanoparticles, is straightforward and economical. Using this technique, we synthesized Zinc Oxide (ZnO) nanoparticles and investigated their characteristics using several characterization techniques. We can regulate the form and size of our nanoparticles by altering the experimental conditions, as demonstrated by our investigations. This demonstrates the importance of experimental parameters in synthesizing ZnO nanoparticles by this ...Более

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Синтез наночастиц меди в присутствии додецилсульфата натрия

Emil ÖMÜRZAK

Методом рентгенофазового анализа показано, что фазовый состав продуктов химического восстановления меди гидразином зависит от условий синтеза и присутствия додецилсульфата натрия. Однофазный продукт, состоящий только из наночастиц меди, синтезируется в аммиачной среде в присутствии додецилсульфата натрия.- Ключевые слова: синтез, наночастицы, медь, химическое восстановление, гидразин, додецилсульфат натрия

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Determination of Acetaminophen in Commercial Formulations Using Silver Nanostructured Aniline Modified Pencil Graphite Electrode

Ali Osman SOLAK

A nanostructured silver-aniline modified pencil electrode obtained by applying experimental design and optimization was developed for the differential pulse stripping voltammetric quantification of acetaminophen in the pharmaceutical products, tablet and syrup. The electrode development process was performed by the modification of PGE with aniline using CV procedure and the reduction of silver nanoparticle on the polyaniline modified PGE. As a result, a new electrode system consisting of a nanostructured silver-polyaniline modified pencil graphite electrode (AgNS-PA-PGE) was obtained to reach ...Более

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Preparation of molecularly imprinted PDMS elastomer for selective detection of folic acid in orange juice

Nahit AKTAŞ

Herein, it is reported an effective method to prepare novel molecularly imprinted polymers (MIP) on poly(dimethylsiloxane) (PDMS) elastomer via a combination of non-covalent imprinting approach and surface initiated reversible addition fragmentation chain transfer (SI-RAFT) polymerization for sensitive and selective detection of folic acid (FA). For this purpose, 2-(2-Methoxyethoxy) ethyl methacrylate (MEOMA), ethylene glycol dimethacrylate (EGDMA), azobisisobutyronitrile (AIBN), FA and dimethylsulfoxide (DMSO) were used as functional monomer, cross-linker, initiator, template molecule, and po ...Более

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Thermal and Optical Properties of In and In2O3 Nanoparticles Synthesized Using Pulsed Plasma in Water

Emil ÖMÜRZAK

We present small indium (In) nanoparticles with an average diameter of 4.5 nm synthesized by pulsed plasma in water. Slightly increased lattice constants and thermal stability of the tetragonal In are revealed by X‐ray diffraction analysis, Rietveld refinement, and thermogravimetric analysis. The highly crystalline body‐centered cubic indium oxide (In2O3) nanoparticles with an average diameter of 12 nm and various shapes (semispherical, semihexagonal, and semicubic) are obtained by annealing the as‐synthesized In nanoparticles at 450 °C. The bandgap energy of the In2O3 nanoparticles is 3.63 eV ...Более

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