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Found: 5 Piece 0.001 sn
Subject Headings : surface modification ✕Researcher : Ali Osman SOLAK ✕
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Prof. Dr. Ali Osman SOLAKMühendislik Fakültesi
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Surface characterization of dinitrophenyl-diaminophenyl nanoplatform on glassy carbon

Ali Osman SOLAK

2,4-dinitrophenol (DNP) was covalently bonded to glassy carbon substrate by cyclic voltammetry (CV) technique. 2, 4-diaminophenol film (DAPO) was acquired with electrochemical reduction of 2,4-dinitrophenol film (DNPO). Prepared films were characterized by X-ray photoelectron spectroscopy (XPS) and germanium attenuated total reflection infrared (GATR-FT-IR) spectroscopy. A hemispherical germanium ATR element used with p-polarized light at 65° incidence angle yielded high signal/noise IR spectra for monolayer coverage of molecules on glassy carbon substrate. Layer thickness of films was measure ...More

Article 2013 Mühendislik Fakültesi Journal of Molecular Liquids187 52 Views
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High energetic body source and strong antioxidant quercetin, morin and rutin: Their covalent grafting onto the glassy carbon electrode surfaces and investigation of surface properties

Ali Osman SOLAK

Herein, electrochemical oxidation and grafting of quercetin, morin and rutin as important biological molecules has been studied with the cyclic voltammetry technique by using a glassy carbon electrode. Electrochemical studies have been performed potentiostatically within a one-compartment three-electrode cell at room temperature. Glassy carbon electrode was used as a working electrode and Pt was used as a wire counter electrode. Ag/Ag+ (10 mM AgNO3), non-aqueous reference electrode calibrated to the E1/2 of ferrocene redox probe and Ag/AgCl/KCl (sat.), an aqueous reference electrode calibrated ...More

Article 2012 Mühendislik Fakültesi Energy Education Science and Technology Part A: Energy Science and Research28 ( 2 ) 89 Views
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1,10-Phenanthroline modified glassy carbon electrode for voltammetric determination of cadmium(II) ions

Ali Osman SOLAK

This study reports the electrochemical modification of glassy carbon (GC) electrode surface with the electro-polymerized form of 1,10-phenanthroline monohydrate (PMH), the characterization of this polyphenanthroline modified electrode (PPMH/GC) and the electroanalytical application suitable for the determination of Cd(II) ions. The PPMH/GC electrode was characterized by cyclic voltammetry, chronoamperometry and atomic force microscopy and formation of polyphenanthroline layer grafted to surface of GC electrode was evidenced. Selectivity of PPMH/GC electrode towards heavy metal ions was investi ...More

Article 2011 Mühendislik Fakültesi Sensors and Actuators B: Chemical157 ( 1 ) 67 Views
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Covalently Grafted on to the Glassy Carbon Electrode in Non-Aqueous Media of Apigenin and Naringenin as Different Flavonoid Derivatives

Ali Osman SOLAK

In this paper, apigenin (AG) and naringenin (NG) have been studied with the cyclic voltammetric technique using the glassy carbon (GC) electrode. The modification was carried out only in non-aqueous media, while the electrochemical characterization was done in both aqueous and non-aqueous media. 0.1 M tetrabutylammonium tetrafluoroborate (TBATFB) in acetonitrile (MeCN) was used in non-aqueous experiments, Britton-Robinson (BR) buffer solution (pH=2) and 0.1 M KCl solution were used in aqueous experiments. Surface modification experiments were performed in the +0.3 V and +2.8 V potential ranges ...More

Article 2011 Mühendislik Fakültesi Analytical and Bioanalytical Electrochemistry3 ( 2 ) 57 Views
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A novel highly sensitive carbon-based HMPD/GC sensor electrode: copper ions analysis in flour and water samples

Ali Osman SOLAK

In this research, (Z)-2-(2-(hydroxyimino)-2-(3-methyl-3-phenylcyclobutyl) ethyl)-3a,7a-dihy-dro-1H-isoindole-1,3(2H)-dione, HMPD molecule has been grafted to the glassy carbon (GC) electrode surface. The HMPD-modified GC electrode has been originally developed and it used for the quantitative determination of Cu(II) in flour and water samples. The modification steps have been performed using cyclic voltammetry (CV). CV, electrochemical impedance spectroscopy and scanning electron microscopy have been employed for the characterization processes. Cu(II) standard solutions changing from 1.0 x 10( ...More

Article 2018 Mühendislik Fakültesi Desalination and Water Treatment112 56 Views
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