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Subject Headings : ferrocenylphosphazen ... ✕Researcher : Ali Osman SOLAK ✕
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Prof. Dr. Ali Osman SOLAKMühendislik Fakültesi
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Phosphorus-nitrogen compounds: part 30. Syntheses and structural investigations, antimicrobial and cytotoxic activities and DNA interactions of vanillinato-substituted NN or NO spirocyclic monoferrocenyl cyclotriphosphazenes

Ali Osman SOLAK

The gradual Cl replacement reactions of NN (1–3) or NO spirocyclic monoferrocenyl cyclotriphosphazenes (4 and 5) with the potassium salt of 4-hydroxy-3-methoxybenzaldehyde (potassium vanillinate) resulted in the mono (1a–5a), geminal (gem-1b–5b), non-geminal (cis-5b and trans -1b–4b), tri (1c, 3c–5c) and tetra-vanillinato-substituted phosphazenes (1d–5d). All the phosphazene derivatives have stereogenic P-center(s), except tetra-substituted ones. The vanillinatophosphazenes have reversible voltammograms with one-electron anodic and cathodic peaks which are attributed to ferrocenyl redox probe. ...More

Article 2015 Mühendislik Fakültesi JBIC : Journal of Biological Inorganic Chemistry20 ( 1 ) 80 Views
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Phosphorus-nitrogen compounds: Part 28. Syntheses, structural characterizations, antimicrobial and cytotoxic activities, and DNA interactions of new phosphazenes bearing vanillinato and pendant ferrocenyl groups

Ali Osman SOLAK

The gradually Cl replacement reactions of spirocyclic mono (1 and 2) and bisferrocenyl cyclotriphosphazenes (3–5) with the potassium salt of 4-hydroxy-3-methoxybenzaldehyde (potassium vanillinate) gave mono (1a–5a), geminal (gem-1b–5b), non-geminal (cis-1b, cis-5b and trans-2b–5b), tri (1c–5c) and tetra-substituted phosphazenes (1d–5d). Some phosphazenes have stereogenic P-center(s). The chirality of 4c was verified using chiral HPLC column. Electrochemical behaviors were influenced only by the number of ferrocene groups, but not the length of the amine chains and the substituent(s). The struc ...More

Article 2013 Mühendislik Fakültesi Journal of Molecular Structure1049 65 Views
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