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Found: 3 Piece 0.002 sn
Department : Kimya Mühendisliği B ... ✕Subject Headings : glassy carbon electr ... ✕
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Modification of glassy carbon electrode by the electrochemical oxidation of 3-aminophenylcalix[4]pyrrole in nonaqueous media

Ali Osman SOLAK

3-Aminophenylcalix[4]pyrrole (3APCP) was grafted to a glassy carbon (GC) surface during the electrochemical oxidation process in 0.1 M tetrabutylammoniumtetra-fluoroborate (TBATFB) containing acetonitrile solution. The presence of a surface film was confirmed electrochemically by comparing voltammograms of dopamine and ferricyanide redox probes at the bare and modified electrodes. Reflection-absorption infrared spectroscopy (RAIRS), XPS, atomic force microscopy (AFM), ellipsometry and the contact angle measurements were also employed to characterize 3APCP film on GC electrode. RAIRS analysis r ...More

Article 2012 Mühendislik Fakültesi Surface and Interface Analysis44 ( 2 ) 59 Views
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Electrochemically grafted etodolac film on glassy carbon for Pb(II) determination

Ali Osman SOLAK

This study reports the electrochemical modification of glassy carbon (GC) surface with etodolac (ETO), the characterization of this ETO modified glassy carbon (ETO/GC) electrode and its electroanalytical application for the determination of Pb(II) ions. Binding type of the etodolac with the glassy carbon surface was investigated and found that it was through the etheric linkage revealed from the reflection–absorption infrared spectroscopy (RAIRS). The ETO/GC electrode was characterized by cyclic voltammetry (CV), reflection–adsorption IR spectroscopy, electrochemical impedance spectroscopy (EI ...More

Article 2012 Mühendislik Fakültesi Sensors and Actuators B: Chemical171-172 74 Views
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1,10-Phenanthroline modified glassy carbon electrode for voltammetric determination of cadmium(II) ions

Ali Osman SOLAK

This study reports the electrochemical modification of glassy carbon (GC) electrode surface with the electro-polymerized form of 1,10-phenanthroline monohydrate (PMH), the characterization of this polyphenanthroline modified electrode (PPMH/GC) and the electroanalytical application suitable for the determination of Cd(II) ions. The PPMH/GC electrode was characterized by cyclic voltammetry, chronoamperometry and atomic force microscopy and formation of polyphenanthroline layer grafted to surface of GC electrode was evidenced. Selectivity of PPMH/GC electrode towards heavy metal ions was investi ...More

Article 2011 Mühendislik Fakültesi Sensors and Actuators B: Chemical157 ( 1 ) 67 Views
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