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Source : Analytical Methods ✕Researcher : Ali Osman SOLAK ✕
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Prof. Dr. Ali Osman SOLAKMühendislik Fakültesi
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A novel apigenin modified glassy carbon sensor electrode for the determination of copper ions in soil samples

Ali Osman SOLAK

In this study, electrochemical modification of a glassy carbon (GC) electrode with apigenin was carried out and the modified electrode was used for determination of copper(II) (Cu(II)) in soil samples. The GC was modified through the electrochemical polymerization of apigenin (PolyApi/GC) on the electrode surface in aqueous media. The electrode surface was modified with apigenin in phosphate buffer solution (PBS), pH 7, from 0 mV to +1400 mV potential ranges, using 100 mV s−1 sweep rate and 30 cycles by cyclic voltammetry (CV). The surface characterizations of this sensor electrode were perfor ...More

Article 2011 Mühendislik Fakültesi Analytical Methods3 ( 11 ) 128 Views
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A novel surface plasmon resonance enhanced total internal reflection ellipsometric application: electrochemically grafted isophthalic acid nanofilm on gold surface

Ali Osman SOLAK

The scope of this study is to modify a Surface Plasmon Resonance (SPR) sensor slide with isophthalic acid to evaluate the possible application on the detection of copper(II) ions in aqueous media by total internal reflection ellipsometry. A gold sensor surface was modified by an electrochemical diazonium reduction modification method. The modified surfaces are characterized with cyclic voltammetry (CV) and ellipsometry. Isophthalic acid monolayer modified gold slides were used for in situdetection of aqueous Cu2+ solution with the SPR enhanced total internal reflection ellipsometry (SPRe-TIRE) ...More

Article 2011 Mühendislik Fakültesi Analytical Methods136 ( 7 ) 75 Views
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