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Publication type : Proceedings Paper ✕Department : Kimya Mühendisliği B ... ✕
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Properties of ZnO and Zn Nanoparticles Produced by Electrical Discharge in Liquid Method

Emil ÖMÜRZAK

The physical processes used to synthesize nanoparticles today are labor-intensive and inefficient in terms of energy use. Our approach, which we employed to create nanoparticles, is straightforward and economical. Using this technique, we synthesized Zinc Oxide (ZnO) nanoparticles and investigated their characteristics using several characterization techniques. We can regulate the form and size of our nanoparticles by altering the experimental conditions, as demonstrated by our investigations. This demonstrates the importance of experimental parameters in synthesizing ZnO nanoparticles by this ...More

Proceedings Paper 2022 Mühendislik Fakültesi International Exchange and Innovation Conference on Engineering and Sciences8 14 Views
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A novel sensitive Cu(II) and Cd(II) nanosensor platform: Graphene oxide terminated p-aminophenyl modified glassy carbon surface

Ali Osman SOLAK

Graphene oxide (GO) based glassy carbon (GC) electrode has been prepared. Firstly, p-nitrophenyl (NP) modified GC (NP/GC) electrode was prepared via the electrochemical reduction of its tetraflouroborate diazonium salt. After the formation of NP/GC electrode, the negative potential was applied to NP/GC electrode to reduce the nitro groups to amine. p-Aminophenyl (AP) modified GC (AP/GC) electrode was immersed into a graphene oxide solution containing 1-ethyl-3(3-(dimethlyamino)propyl)-carbodiimide. Hence, we constructed GO terminated AP modified GC (GO/AP/GC) electrode. NP/GC, AP/GC and GO/AP/ ...More

Proceedings Paper 2013 Mühendislik Fakültesi Electrochimica Acta112 78 Views
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Synthesis of Nanomaterials by the Pulsed Plasma in Liquid and their Bio-medical Applications

Emil ÖMÜRZAK | Ruslan ADİL AKAY TEGİN

Pulsed plasma in liquid is a simple, ecologically friendly, cost-efficient method based on electrical discharge between two metal electrodes submerged into a dielectric liquid. We synthesized carbon-encapsulated Fe (Fe@C) magnetic nanoparticles with low cytotoxicity using pulsed plasma in a liquid. Body-centered cubic Fe core nanoparticles showed good crystalline structures with an average size between 20 and 30 nm were encapsulated in onion-like carbon coatings with a thickness of 2–10 nm. Thermal gravimetric analysis showed a high stability of the as-synthesized samples under thermal treatme ...More

Proceedings Paper 2018 Mühendislik Fakültesi 2017 International Conference on Aerospace Technology, Communications and Energy Systems (ATCES 2017)302 ( UNSP 012076 ) 94 Views
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Copper Nanoparticles: Synthesis and Biological Activity

Emil ÖMÜRZAK | Tinatin DOOLOTKELDİEVA | Saykal BOBUŞOVA

By means of XRD and FESEM analysis, it is established that copper nanoparticles with sizes less than 10 nm are formed during the chemical reduction, which form aggregates mainly with spherical shape. Presence of gelatin during the chemical reduction of copper induced formation of smaller size distribution nanoparticles than that of nanoparticles synthesized without gelatin and it can be related to formation of protective layer. Synthesized Cu nano-powders have sufficiently high activity against the Erwinia amylovora bacterium, and the bacterial growth inhibition depends on the Cu nanoparticles ...More

Proceedings Paper 2018 Mühendislik Fakültesi 2017 International Conference on Aerospace Technology, Communications and Energy Systems (ATCES 2017)302 ( UNSP 012075 ) 187 Views
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Preparation of stabilized silver and tin nanocomposites by electrical discharge

Emil ÖMÜRZAK

In this study silver and tin nanocomposites were synthesized by electro spark dispersion in ethanol. Resulting nanocomposite was characterized by using the powder x-ray diffraction and emission scanning electron microscopy. It was found by X-ray phase analysis that the product obtained by electro spark joint dispersion of silver and tin in ethanol consists of two phases: Ag3Sn and beta-Sn. The results of processing SEM micrographs of the product of the Ag-Sn system show that the obtained phases are spherical nanostructures with sizes of 30-60 nm. This size of nanostructures was associated wit ...More

Proceedings Paper 2020 Mühendislik Fakültesi MATERIALS TODAY-PROCEEDINGS31 ( Part 3 ) 103 Views
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Effect of surfactant materials to nanoparticles formation under pulsed plasma conditions and their antibacterial properties

Emil ÖMÜRZAK | Ruslan ADİL AKAY TEGİN

Pulsed plasma between two Zn rods submerged into aqueous solution of cetyl trimethylammonium bromide (CTAB) and sodium dodecyl sulphate (SDS) surfactants resulted in formation of pure ZnO nanorods, while the pulsed plasma between two Zn rods in water without surfactant yielded a mixture of ZnO and Zn nanoparticles. Carbon coated ZnO nanorods with about 20 nm thickness and 150 nm length were synthesized by this method using different surfactant materials such as CTAB and SDS. Cu nanoparticles of about 10 nm in size were also synthesized by the pulsed plasma in aqueous solution of 0.2 % gelatine ...More

Proceedings Paper 2018 Mühendislik Fakültesi Materials Today: Proceedings5 ( 7-3 ) 106 Views
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