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3-Aminophenylcalix[4]pyrrole (3APCP) was grafted to a glassy carbon (GC) surface during the electrochemical oxidation process in 0.1 M tetrabutylammoniumtetra-fluoroborate (TBATFB) containing acetonitrile solution. The presence of a surface film was confirmed electrochemically by comparing voltammograms of dopamine and ferricyanide redox probes at the bare and modified electrodes. Reflection-absorption infrared spectroscopy (RAIRS), XPS, atomic force microscopy (AFM), ellipsometry and the contact angle measurements were also employed to characterize 3APCP film on GC electrode. RAIRS analysis r ...More
Herein, electrochemical oxidation and grafting of quercetin, morin and rutin as important biological molecules has been studied with the cyclic voltammetry technique by using a glassy carbon electrode. Electrochemical studies have been performed potentiostatically within a one-compartment three-electrode cell at room temperature. Glassy carbon electrode was used as a working electrode and Pt was used as a wire counter electrode. Ag/Ag+ (10 mM AgNO3), non-aqueous reference electrode calibrated to the E1/2 of ferrocene redox probe and Ag/AgCl/KCl (sat.), an aqueous reference electrode calibrated ...More