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A novel molecularly imprinted polymer was synthesized on magnetic halloysite nanotube via surface initiated reversible addition-fragmentation chain transfer polymerization in the presence of 2-aminoethylmethacrylamide, 2-Cyano-2-propyl benzodithioate, ethylene glycol dimethacrylate (EGDMA) and azobis(isobutyronitrile) for sensitive and selective spectrophotometric determination of metoclopramide in urine samples. The synthesized imprinted polymer was characterized by several surface characterization techniques and the results indicated there was a thin polymer network on the magnetic halloysit ...Более
In this study a novel and smart multi-functional hydrogel (MFH) was synthesized from N, N dimethyl acrylamide (DMAAm), gelatin, citric acid (CA) and pomegranate extract (PE) for instant and easy monitoring of the color change in MFH due to changes in medium conditions such as pH and temperature. MFH was utilized as food packaging material, equipped with the developed properties. MFH was synthesized with a redox polymerization technique in film form on petri dishes. Mechanical and water resistance properties of MFH were improved by CA and N, N, methylenebisacrylamide, while PE was used to gain ...Более
In this study, magnetic metal nanoparticles (MNP) were prepared by using Fe, Co and Ni ions and NaBH4 as reducing agents in oil-in-water microemulsion system. The prepared MNP were used as catalyst in 4-Nitro phenol (4-NP) reduction to 4-Aminophenol (4-AP). It was found that magnetic Co MNP performed superior catalytic performances than Fe and Ni MNP for 4-NP reduction. The catalytic reduction experiments revealed that as the concentration of reducing agent, NaBH4 that was used in the preparation of Co MNP was increased, the complete conversion time for 4-NP to 4-AP was decreased as the sizes ...Более
Novel biocompatible homo and co-polymeric microparticles were synthesized from maleic acid (MA) and citric acid (CA) for uptake/release thiamine as a model drug. Surfactant-free self-emulsion polymerization technique was accomplished to synthesize the microparticles in a single step. The antimicrobial, antioxidant properties of those microparticles and their thiamine uptake/release capacities were investigated. Fourier transform infrared spectroscopy (FTIR), thermogravimetric analyzer (TGA), particle-size/zeta-potential (Zeta/DLS) and scanning electron microscopy (SEM) instruments were utilize ...Более
In this study, it was aimed to investigate the synthesis, characterization and drug release behaviors of organohydrogels containing pH-sensitive Agar (A), Glycerol (G), Thyme Oil (TO). The novel organo-hydrogels containing TO were prepared in an emulsion media by the free-radical polymerization and crosslinking reactions among Agar (A), Glycerol (G), TO, N, N, methylenebisacrylamide (MBA) or glutaraldehyde (GA) reagent. Swelling ability (ethanol, acetone, ethanol/ID water (1:1), acetone/ID water (1:1) and gasoline environments and different pH), Fourier Transform Infrared Spectroscopy (FTIR) a ...Более