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New Voltammetric Approach to the Quantitative Estimation of Sildenafil Citrate in Tablets Using Disposable Pencil Graphite Electrode

Ali Osman SOLAK

The voltammetric behavior of sildenafil citrate (SC) was studied through differential pulse stripping voltammetry. The best sensitivity, optimal experimental conditions and settings for the voltammetric method development were obtained by applying experimental design and optimization methodology to the designed sample runs at different accumulation times, accumulation potentials and pHs. The linearity over the concentration range 1 × 10–7 M–8 × 10–6 M for SC was determined and the limit of detection (LOD) was 3.1 × 10–8 M. For the method ability and validity, mean recovery result and relative ...Более

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Experimental analysis of energy, performance and noise emissions for biodiesel fuel obtained from animal waste fat

Hüseyin ÖĞÜT

Animal fats are one of the biodiesel raw materials. In this study, biodiesel was produced from horse fat by transesterification method and the produced biodiesel was mixed with euro diesel at 5 by volume, and experimental fuels in the form of D-100 and D95B5 were obtained. Fuel properties of test fuels were determined. In addition, using the experimental fuels in a single-cylinder, four-stroke, water-cooled diesel engine, the data obtained by investigating the engine performances, energy analysis, and noise emissions were presented with graphics and interpreted. In the experiment results; D95B ...Более

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Effects of using ethanol-biodiesel-diesel fuel in single cylinder diesel engine to engine performance and emissions

Hüseyin ÖĞÜT

In this study, biodiesel was produced from safflower seeds by converting the raw oil obtained through dampening them via the rolling process, roasting at 90 °C and pressing into Safflower Oil Methyl Esther (Safflower Biodiesel) using the trans-esterification method. Experimental fuels were obtained in the forms of D100, B2.5M2.5D95, B5M5D90, B5M2.5D92.5 and B2.5M5D92.5 by mixing the biodiesel fuel obtained from safflower with diesel fuel, adding bio-ethanol at the rates of 2.5% and 5%, and volumetrically in inverse ratio. Tests were conducted to determine the fuel properties of the mixed fuels ...Более

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