Thermal and Optical Properties of In and In2O3 Nanoparticles Synthesized Using Pulsed Plasma in Water

Emil ÖMÜRZAK

We present small indium (In) nanoparticles with an average diameter of 4.5 nm synthesized by pulsed plasma in water. Slightly increased lattice constants and thermal stability of the tetragonal In are revealed by X‐ray diffraction analysis, Rietveld refinement, and thermogravimetric analysis. The highly crystalline body‐centered cubic indium oxide (In2O3) nanoparticles with an average diameter of 12 nm and various shapes (semispherical, semihexagonal, and semicubic) are obtained by annealing the as‐synthesized In nanoparticles at 450 °C. The bandgap energy of the In2O3 nanoparticles is 3.63 eV ...Daha fazlası