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Erişime Açık

Promoting formic acid and ethylene glycol electrooxidation activity on Ga modified Pd based catalysts

Hilal DEMİR KIVRAK | Nahit AKTAŞ

Herein, carbon nanotube (CNT)-supported Ga@PdAgCo catalysts were synthesized by sodium borohydride (SBH) sequential reduction method. These catalysts were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), X-ray photoelectron spectroscopy (XPS), and inductively coupled plasma-mass spectrometry (ICP-MS). Characterization results revealed that these catalysts were succesfully preared at desired loading and atomic ratios. From the XRD pattern, the crystallite size of 0.5 Ga@PdAgCo(80:10:10)/CNT catalysts was found as 6.95 nm by utilizing the Scherrer equation. From ...Daha fazlası

Erişime Açık

The effect of titanium dioxide-supported CdSe photocatalysts enhanced for photocatalytic glucose electrooxidation under UV illumination

Nahit AKTAŞ

The wetness impregnation method was used to synthesize 0.1 CdSe/TiO2 photocatalysts with different atomic molar ratios (90-10, 70-30, 50-50, and 30-70). These catalysts were characterized by XRD, SEM-EDX and mapping, TEM-EDS, UV-VIS spectroscopy, fluorescence spectroscopy, XPS, TPR, TPO, and TPD analyses. Cyclic voltammetry (CV), chronoamperometry (CA), and electrochemical impedance spectroscopy (EIS) analyses were performed to examine the photocatalytic activity for photocatalytic fuel cells (PFCs) in glucose solution in the dark and under UV illumination. The characterization analyses reveal ...Daha fazlası

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